4,4′,6,6′-Tetra­hydro­seleno-2,2′-[(E,E)-cyclo­hexane-1,2-diylbis(nitrilo­methyl­idyne)]diphenol

نویسندگان

  • Qiang Wang
  • Ru-Hua Zha
  • Ji-Wen Yuan
  • Qing-Fu Zeng
چکیده

In the title mol-ecule, C(20)H(22)N(2)O(2)Se(4), the dihedral angle between the pendant aromatic rings is 67.1 (2)°. The conformation is stabilized by two intra-molecular O-H⋯N hydrogen bonds.

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منابع مشابه

(R,R)-4,4′-Dibromo-2,2′-[cyclo­hexane-1,2-diylbis(nitrilo­methyl­idyne)]diphenol

The mol-ecule of the title compound, C(20)H(20)Br(2)N(2)O(2), lies on a twofold axis. It contains two stereogenic C atoms with R chirality and thus it is the enatiomerically pure R,R-diastereomer. There is an intra-molecular O-H⋯N hydrogen bond.

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In the title complex, [Fe(C(22)H(24)N(2)O(4))]·H(2)O, the Fe(II) center is four-coordinated by two O and two N atoms from 2,2'-[6,6'-dimethoxy-cyclo-hexane-1,2-diylbis(nitrilo-methyl-idyne)]diphen-olate (L) ligands in a distorted square-planar geometry. Uncoordinated water and FeL mol-ecules are paired via inter-molecular water-meth-oxy O-H⋯O hydrogen bonds.

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6,6′-Dimeth­oxy-2,2′-[(cyclo­hexane-1,2-di­yl)bis­(nitrilo­methyl­idyne)]diphenol

The mol-ecule of the title compound, C(22)H(26)N(2)O(4), has two azomethine linkages, both of which are in an E configuration. The cyclo-hexyl ring adopts a chair conformation. The dihedral angle between the benzene rings is 66.57 (9)°. The mol-ecular structure is stabilized by two intra-molecular O-H⋯N hydrogen bonds.

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6,6′-Dimeth­oxy-2,2′-[pyridine-2,3-diylbis(nitrilo­methyl­idyne)]diphenol

In the title compound, C(21)H(19)N(3)O(4), two intramolecular N-H⋯O hydrogen bonds generate two six-membered rings. The dihedral angles between the central heterocyclic ring and the two pendant rings are 61.5 (2) and 63.5 (1)°.

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Bis{μ-4,4′-dimeth­oxy-2,2′-[propane-1,2-diylbis(nitrilo­methyl­idyne)]diphenolato}bis­({4,4′-dimeth­oxy-2,2′-[propane-1,2-diylbis(nitrilo­methyl­idyne)]diphenol}manganese(III)) bis­(hexa­fluorido­phosphate)

In the title complex, [Mn(2)(C(19)H(20)N(2)O(4))(2)(C(19)H(22)N(2)O(4))(2)](PF(6))(2), the Mn(III) ion is coordinated by two O [Mn-O = 1.855 (2) and 1.887 (2) Å] and two N [Mn-N = 1.982 (3) and 1.977 (3) Å] atoms from the tetra-dentate Schiff base ligand and a coordinated axial ligand [Mn-O = 2.129 (2) Å]. The centrosymmetric dimer contains two Jahn-Teller-distorted Mn(III) ions, each in a near...

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عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009